SYKAM S 4011 Column Thermo Controller

  • Technical Specifications
  • Temp. Element: Integrated Peltier Elements
  • Chamber Size: 35 x 35 x 300 mm
  • Temp. Range: +5° C to +70° C
  • Temp. Accuracy: ±0.5° C
  • Temp. Constancy: ±0.1° C
  • Temp. Selection: 1° C steps
  • External Control: analoge control
  • Display: 2-digit 7-segment
  • Safety Features: Gas Sensor f. flammable gases, overheat protection
  • Dimensions: Controller: 220x150x345mm, Oven: 135x180x510mm
  • Power: 110/220 V, 50/60 Hz
  • Weight: Controller: 6.3 kg, Oven: 9.4 kg

 S_4011

Not only the optimization of separations but also a constant temperature of the eparation column plays a very important role in the reproducibility of the

retention times. The Column Thermo Controller S 4011 was especially developed in order to overcome these kind of problems. With the help of the built-in Peltier elements, it is ossible to keep the temperature of the columns between +5° C and +70° C independent of the ambient temperature.

A precise column cooling system for programmable fluorescence detection and for the optimization of later eluting components is of great advantage. Especially separations which are very temperature dependent, like gradient elution of polycyclic aromatic hydrocarbons, greatly profit by this instrument.

The integrated Peltier elements provide exact temperature control. Therefore, fast temperature changes are possible, which are needed for temperature gradients.

Furthermore, the Column Thermo Controller S 4011 can not only be used for heating, but also for cooling below ambient temperature.

 

Gas Sensor Safety Feature

At the inside of the column chamber a gas sensor is installed for detecting flammable gases. Should there be a leakage during operation, the yellow LED will indicate the leakage and the oven is automatically switched off.

S-4011_innen

Cat.-No. Description

10 40 007 S4011 Column Thermo Controller

The FS 160 possess various triggering possibilities. Beside the impulse- and time-control the fraction collector can gather the flow quantity of the pump and thus collect an adjustable volume per fraction. By exchanging the pieces of drop in the parallel chromatography up to 10 channels can be fractioned at the same time.
Customer-specific tanks can be integrated by simply adjusting the rack parameters. With the optionally available waste/fraction valve unused chromatography parts can be disposed in a larger storage tank.FS160
Additionally the valve is operated during each glass change. A marker indicates the fraction change in the chromatogram.
FS160

FS 1000 Large volume Fraction Collector
FS1000
- XY Fraction Collector Completly SS and movable
- Z-optional
- Standard vial size of 0,5 L (60 flasks) or 1,0 L (40 Flasks)
- Impuls-, Time- or Volume
- Waste-/Fraction Valve
- BESTA-Pomps Integrated (Start/Stop/Flow)
- Also run as manual

FS24
- 24 postion Fraction Collector: high flow
- Variable volumes

SYKAM Data System: Clarity

Clarity is an advanced chromatography station designed to acquire and evaluate data from up to four chromatographs at a time. Clarity - a top product in its category - represents a universal solution for laboratories. It enables the user to acquire data from any commercially available chromatograph with standard analogue output.

Up to four chromatography systems, each of which can be equipped with up to four detectors, can be connected simultaneously. The chromatography station package includes an A/D converter (internal PCI card or external USB box) and the corresponding Clarity Software.

 

Support for GLP/ 21 CFR Part 11

In recent years, chromatography practice has brought about not only the necessity of efficiency in laboratory work, but also new demands relating to monitoring

and security mechanisms, particularly in the field of data management. The Clarity supporting tools help you to comply with the requirements of GLP (Good

Laboratory Practice) and FDA - 21 CFR Part 11.

Data Security

A system of access rights and passwords is set up within the station. This system allows to create a unique password protected profile for each user.The user profile then defines in detail the user’s rights within the station (e.g. authority to effect changes in the methods of measurement) and may limit ones access to only certain connected instruments. Electronic signatures are also incorporated into the

system so that a user may sign his or her data. This electronic signature is stored with the name and date and supplemented with a set phrase (e.g. measured

by, approved by, etc.).

Audit Trail

Detailed logs and histories of modifications enable users to maintain an audit trail. Clarity documents all parameters describing the conditions and methods of data processing for the user. This allows for easy access to a complete profile of information regarding any prior modification’s performance.

 

Qualification Tools

The Test IQ (Installation Qualification) is an integral component of the station. This test monitors that the software has been properly installed and the results can be accessed from a printed protocol. Clarity Validator for OQ (Operational Qualification) is an optional package available for testing and validating the Clarity chromatography station.This is accomplished simply with the use of our chromatogram generator and a software utility.

 

U-PAD - External USB A/D Converter

The U-PAD is an external measuring unit for acquisition of data from detectors with standard analog output. U-PAD uses a USB communication channel, which allows direct connection from the PC. U-PAD represents an ideal solution for connecting chromatographs to a laptop computer. The unit contains two independent channels equipped with the latest 24-bit A/D converters, which attain higher effective resolution, particularly at higher integration frequencies and lower voltage ranges. The channels are isolated with symmetrical inputs.

 

Software Features

 

Algorithm for Detection of Peaks

Highly responsive algorithms enable users to detect hundreds of peaks in each hromatogram. Data from the analysis can naturally be reprocessed without the necessity of repeating the analysis.

 

Integration

All integration parameters are saved in the integration table. Parameters such as Peak Width and Threshold are programmable in time. There are a total of 27 integration parameters incorporated to ensure the optimal integration of peaks.

Most of these parameters can be applied also with the mouse from icons on the toolbar. Every change of basic integration parameters in the chromatogram window will force immediate reintegration.

 

Method

All parameters for data acquisition and peak integration, including baseline operations and link to the calibration file are saved in the template method. After

creating of a chromatogram, a copy of the template method becomes a part of the chromatogram file.

 

Multi-Detector Measurement

Once a measurement has been completed within the framework of one instrument and more than one detector (up to four), signals are simultaneously displayed

and accompanied by a legend identifying each signal and detector. Users may select the number of signals displayed according to preference.

 

Calibration

The Clarity Station uses linked calibration. Calibration curves are saved in a separate file, to which the template and chromatogram methods are referring. After updating or modifying this calibration file, results in all chromatograms linked to this file will be

automatically recalculated upon opening. Although the calibration is linked, the current states of the calibration file and methods are stored in the chromatogram every time it is saved (using the commands Save, Print or Export).

The chromatogram with its former method settings and calibration curves may thus be opened from any prior saved state.

 

Calibration Calculations

Clarity offers the ability to calculate using external or internal standard methods.

There are six types of curves to fit calibration points with the option to include a zero point. The station allows you to select automatic or manual (interactive) method of data transmission from the calibration standard into the calibration file. Groups

of peaks may also be calibrated.

 

Method of Reference Peak

Use reference peaks and or customizable identifi-cation windows for individual peaks to enhance the accuracy of compound identification.

Editing and Calibration

Browsing and adjustment of calibration data is simple thanks to the consolidation of all compounds in a single global calibration table.

 

Print Protocols

The Clarity station supports printing of user defined protocols. Its configuration is saved in report style, which defines the content and form of the printout. Pick from the predefined report styles or adjust them and store for further use. Different report styles can be predefined according to the dialog in which you are working.

You can review the printout on the screen in the print preview. For printing protocols from multiple analyses users can either use batch processing of data or print a

summary table.

 Chemyx Syringe Pumps 

All Systems Spec's:

◦ high-precision fluid dosing

◦ wide flow ranges

◦ syringe manufacturer independent

◦ constant and variable flow

◦ USB, RS232, TTL for PC control

Accuracy: ± 0.35%

Reproducibility: ± 0.05%


 Fusion 100

Fusion Touch 100

Infusion-only system designed for precise laboratory fluid delivery.

  1. Flow rates: 0.0001µl/min to 102ml/min
  2. Accepts syringes up to 60ml
  3. Infusion only

Flow Rate:

Minimum: (10μl syringe) 0.0001 μl/min
Maximum: (60 ml syringe) 102 ml/min
Linear Force: 35 lbs with variable force selection
Step Resolution: 0.098 microns


Fusion 200

Fusion 200

Infuse/Withdraw modular system, for flexible dosing configurations up to 10 syringes.

  1. Flow rates: 0.0001µl/min to 65ml/min
  2. Accepts syringes up to 60ml
  3. Infuse and Withdraw

Flow Rate:
Minimum (10μl syringe): 0.0001 μl/min
Maximum (60 ml syringe): 61 ml/min
Linear Force: 50 lbs with variable force selection
Step Resolution: 0.046 microns


Fusion 400

Fusion 400

Infusion-only with high volumetric accuracy for microfluidics and microdialysis use.

  1. Flow rates: 0.00001µl/min to 10ml/min
  2. Accepts syringe up to 10ml
  3. Infuse only

Flow Rate:
Minimum (0.5 μl syringe): 2 pl/min
Maximum (10 ml syringe): 10 ml/min
Linear Force: 50 lbs with variable force selection
Step Resolution: 0.016 microns

Spec's for all Fusion Touch systems:

Height: 4.5 inches (114mm)
Width: 9.5 inches (241mm)
Depth: 6.5 inch (165mm)
Weight: 7lbs (3kg)

Free USB 2.0 port or RS232 COM port
Windows: XP, VISTA, 7
Mac: Mac OS X v10 or later
Linux (call for drivers and supported versions)

RS232: Straight-through D9 Female Receptacle
USB: USB Type B Male Receptacle
TTL I/O: USB Type B Receptacle

CE, UL, CSA, RoHS, FCC

Operating Temperature: 4°C to 40°C (40°F to 104°F)
Storage Temperature: -10°C to 70°C (14°F to 158°F)
Humidity: 20% to 80% RH, non-condensing 

 

 

◦ high precision fluid dosing

◦ instantaneous flow stability

◦ high pressure capabilities

◦ constant and variable flow

◦ USB, RS232, TTL for PC control

 

Nexus 3000

Nexus 3000 :Highly versatile syringe pump with instantaneous flow stabilization
Flow rates: 0.00001µl/min to 300ml/min

  1. Accepts syringes up to 140 ml
  2. Infuse and Withdraw
  3. 10-channel and push/pull rack options

The Nexus series syringe pumps are high-end fluid delivery systems designed to tackle extremely tough applications with high rate variation sensitivities due to high pressure and viscosity dosing.

Standard Features:

•Color Graphic LCD interface
•RS232 port standard for computer control
•Infuse/withdraw rack
•Gradient/multistep pumping function
•Stall detection

Users can program in (without a PC):
Constant flows
Variable/Punctuated flow profiles
Gradient flows
Advanced loops
*Or mix and match in our highly flexible interface.

The Nexus 3000 syringe pump has high instantaneous flow stability with less than 8% of the nominal flow in nanoliter ranges for critical rate variation sensitive experiments. No other syringe pump system can come near these sub-microliter flows. Please ask SD about this capability and option.

This system has a variable transmission that gives this unit the largest flow range of any syringe pump on the market. This system can "shift gears" to reach low picoliter rate and high 500ml/min rates - almost a 12 order magnitude difference.

The Nexus 3000 syringe pump can be equipped with a push/pull rack and a 10-channel infuse/withdraw rack.

Flow Rate Nexus 3000:

Minimum (0.5 μl syringe): 1.56 pl/min
Maximum (140ml syringe): 300 ml/min
Linear Force: 65 lbs
Step Resolution: 0.012 microns

All Systems:
Accuracy: ± 0.35%
Reproducibility: ± 0.05%


The Nexus 6000

 

Standard Features:

•450 lbs avg force up to 550 lbs max force •RS232 port for PC control
•Gradient/multistep pumping function standard •Stall detection with audible alarm

 

Nexus 6000

The Nexus 6000 is the most powerful high pressure syringe pump on the market with 450 lbs average pushing force up to 550 lbs max force. This system has a steel brace mechanism with a bolt lock ensuring long pump life span under high stress.

RS232 and TTL come standard on every Nexus syringe pump. This system not only takes commands from PCs, it can also be controlled from PLCs and NI cards. Commands are formatted in easy-to-understand ASCII text that can be sent by an array of programs from Labview, Labwindows, Visual Studio, MatLab and Hyperterminal, to name a few. Every system also comes with a free Windows-based pump controller program for easy computer control.

Stainless Steel Syringes Available

The Chemyx also offers a wide selection of stainless steel syringes. These syringes come with standard NPT thread design that are directly compatible a variety of standard Swagelok fittings. Please see the stainless steel syringes here.

Flow Rate Nexus 6000:
Minimum (0.5 μl syringe): 1.56 pl/min
Maximum (200 ml syringe): 200 ml/min
Linear Force: 450-550 lbs (self adjusting)
Step Resolution: 0.046 microns
4.3 inch (diagonal) wide screen color LCD

Spec's for all Nexus systems:

Height: 6 inches (152.4 mm)
Width: 10.5 inches (266.7 mm)
Depth: 8 inch (203.2 mm)

Weight: 13lbs

RS232 COM port
Windows: XP, VISTA, 7
Mac: Mac OS X v10 or later
Linux (call for drivers and supported versions)

RS232: Straight-through D9 Female Receptacle
TTL I/O: Straight-through D9 Female Receptacle

CE, UL, CSA, RoHS, FCC

Operating Temperature: 4°C to 40°C (40°F to 104°F)
Storage Temperature: -10°C to 60°C (14°F to 158°F)
Humidity: 20% to 80% RH, non-condensing


Hybrid Touchscreen and Keypad Interface

Set any parameter through a familiar "windows" like environment and change settings from syringe ID, flow rate, volume, and delay time. Syringe dimensions can also be loaded from an internal syringe library stored on the pump. Dual entry modes allow users to wear gloves and still operate the system.

Both keypad and screen are coated with solvent-resistant PP coating for operational durability under laboratory environments.

Touch Screen

The new Fusion touch syringe pump has one of the newest ARM processors, allowing it to load/save methods, control motor force, and run an array of complex flow profiles.

 Touch Screen

Users can program in (without a PC):
Constant flows
Variable/Punctuated flow profiles
Gradient flows
Advanced loops
*Or mix and match in our highly flexible interface.


Spring-Loaded Syringe Clamps

Fushion Holder


10-Channel Infuse/Withdraw Rack

The Fusion 200 has an optional modular 10-channel infuse/withdraw rack. The rack is removable and can hold syringes up to 10ml.

Fushion 10 Holder


Base controller for Nanojet system with up to four connections to headers.

- Keypad Interface 

- Accepts up to 4 headers

- Controllable via RS232

 

 Stereotaxic Modular Syringe Pump-

Remote Syringe Pump Module

Nano Module

Four pump headers can be equipped and controlled by one pump control box. The headers are capable of delivering very finite amounts of drug to parts of the brain or for use in microdialysis.

The Nanojet header is shielded and can be used with MRI machines up to the 500 gauss line.
The Nanojet syringe pump is a sensitive modular stereotaxic syringe pump for use in surgery and to handle radioactive material. The header is a small syringe pump - weighing only 525 grams and can be detached and placed away from the control box while connected with a CAT 5 cable. This syringe pump infuses/withdraws microsyringes, and can infuse glass and plastic syringes up to 2ml.

 

 

SYKAM S 7505/7510 Vacuum Degasser

The degassing of solvents is very important in liquid chromatography, as oxygen and other in the solvent dissolved gases affect the analysis for various reasons; through the volume contraction (gradient mixing), different pressure ratio (in front and behind the column) and caused by different temperatures, the dissolved gases are released in course of time. This will influence the reliability of the analysis (pump) as well as the detection efficiency (measuring cell). Therefore, dissolved gases have to be removed from the solvent.

Operation Principle of the Degasser In a vacuum chamber, the solvent to bedegassed is distributed into several, parallel arranged, semi-permeable membrane chambers. When a high vacuum (more than -850 mbar) is applied, only the in the liquid dissolved gases are diffusing through the thin membrane. With a total solvent volume of 8 ml per degassing channel, the Sykam Degasser S 7510 achieves an extremely low remaining gas concentration of 0.5 to 5 ppm oxygen, depending on the degasser‘s flow rate (0 to 10 ml/min). With a given flow rate, the degassing quality can be further increased by coupling two or several membrane channels.degassing

The digital display of the actual vacuum in Milibar makes the Sykam Degasser S 7510 the first vacuumt. degasser on the market which functions can be checked and documented at any time.  On top of that, the actual vacuum run can be continuously registered via an analogue DC output (-1 V for 1000 mbar). Through in integrated logic, any leakage in the vacuum system is detected (run time of the vacuum pump for defined vacuum range) and is not only optically displayed by a controll LED but is also indicated through a relay contact closure for peripheral systems. For removing possibly existing solvent traces, the vacuum pump‘s waste gases can be directed via a fixable tube connection to the laboratory‘s ventilation. The Teflon membrane packages are exchangable, in case of damage.

S7510

Technical Specifications

  • Degassing Method: Applied Vacuum
  • Efficiency: 0.5ppm oxygen
  • Flow Rate: max. 10 ml/min
  • Volume/Channel: 8 ml
  • Display: 4-character
  • Dimensions: 110 x 150 x 350 mm
  • Power: 110/220 V, 50/60 Hz
  • Weight: 5.6 kg

Cat.-No. Description

10 71 001 S 7510 Degasser, 2-Channel

10 71 002 S 7510 Degasser, 3-Channel

10 71 003 S 7510 Degasser, 4-Channel

10 71 004 S 7505 Degasser, 2-Channel

10 71 005 S 7505 Degasser, 3-Channel

10 71 006 S 7505 Degasser, 4-Channel


SYKAM S 7131 Reagent Organizer

The S 7131 Reagent Organizer is the optimal solution for storing your solvents. The integrated gas supply with pressure regulator let you store the eluent under inert-gas pressure, or for degassing purposes using Helium. The organizer can hold up to four eluent bottles, which can be closed indivdually with the integrated valve bottle caps. The S 7131 Reagent Organizer could be used with the S 2100 Solvent Delivery System.

S7131

  • Gas Pressure: 0 to 7 bar
  • Eluent Supply: 1 to 4 solvent bottles
  • Dimensions: 480 x 310 x 350 mm
  • Weight: ~7 kg

 

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